Table 2 The NMR (400 MHz) data of the compound (2)
Compound (2) | Literature Data (Hoskovec et al. 1990) | |||||
|---|---|---|---|---|---|---|
Position | 1H (ppm) | 13C (ppm) | DEPT | 1H (ppm) | 13C (ppm) | DEPT |
C-1 | 4.57 (d, 2H) | 66.28 | CH2 | 4.20 (d, 2H) | 58.61 | CH2 |
C-2 | 5.90 (m, 1H) | 129.86 | CH | 5.54 (m, 1H) | 128.26 | CH |
C-3 | 5.80 (m, 1H) | 132.41 | CH | 5.67 (m, 1H) | 133.28 | CH |
C-4 | 2.28 (m, 2H) | 27.35 | CH2 | 2.02 (m, 2H) | 27.43 | CH2 |
C-5 | 1.21 (m, 2H) | 29.94 | CH2 | 1.22 (m, 2H) | 29.75 | CH2 |
C-6 | 1.35 (m, 2H) | 29.71 | CH2 | 1.39 (m, 2H) | 29.60 | CH2 |
C-7 | 1.29 (m, 2H) | 29.62 | CH2 | N.L | 29.55 | CH2 |
C-8 | 1.16 (m, 2H) | 29.55 | CH2 | N.L | 29.52 | CH2 |
C-9 | 1.27 (m, 2H) | 29.43 | CH2 | N.L | 29.47 | CH2 |
C-10 | 1.37 (m, 2H) | 29.32 | CH2 | N.L | 29.44 | CH2 |
C-11 | 1.19 (m, 2H) | 29.21 | CH2 | 1.21 (m, 2H) | 29.28 | CH2 |
C-12 | 2.17 (m, 2H) | 24.81 | CH2 | 2.02 (m, 2H) | 26.91 | CH2 |
C-13 | 5.53 (m, 1H) | 130.16 | CH | 5.28 (m, 1H) | 129.83 | CH |
C-14 | 5.55 (m, 1H) | 130.16 | CH | 5.43 (m, 1H) | 129.83 | CH |
C-15 | 2.17 (m, 2H) | 27.29 | CH2 | 2.02 (m, 2H) | 27.19 | CH2 |
C-16 | 1.21 (m, 2H) | 32.06 | CH2 | 1.22(m, 2H) | 31.96 | CH2 |
C-17 | 1.43 (m, 2H) | 22.88 | CH2 | 1.39 (m, 2H) | 22.34 | CH2 |
C-18 | 0.83 (t, 3H) | 14.23 | CH3 | 0.90 (t, 3H) | 13.99 | CH3 |
OH | 5.21 (s, 1H) | 5.21 (s, 1H) | ||||